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Updated: Jun 23, 2026

Synthesis and Performance Characterizations of Transition Metal Single Atom Catalyst for Electrochemical CO2 Reduction
Published on: April 10, 2018
Carbon nanotubes, phthalocyanines and porphyrins: attractive hybrid materials for electrocatalysis and
José H Zagal1, Sophie Griveau, Kenneth I Ozoemena
1Departamento de Química de los Materiales, Facultad de Química y Biología, Universidad de Santiago de Chile, Casilla 40, Correo 33 Santiago, 917 0022, Chile.
Abstract:
The manuscript discusses different ways of forming hybrid materials between single (SWCNT) or multi (MWCNT) walled carbon nanotubes and biomimetic compounds such as metalloporphyrins, metallophthalocyanines and other MN4 complexes. The hybrid materials are employed for electrocatalysis of reactions such as oxygen and hydrogen peroxide reduction, nitric oxide oxidation, oxidation of thiols and other pollutants. Methods of characterizing the hybrid materials such as cyclic voltammetry (CV), scanning electron microscopy (SEM), transmission electron microscopy (TEM), X-ray photoelectron spectroscopy (XPS), atomic force microscopy (AFM) and scanning electrochemical microscopy (SECM) are discussed.
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