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Corrected direct force balance method for atomic force microscopy lateral force calibration.

David B Asay1, Erik Hsiao, Seong H Kim

  • 1Department of Chemical Engineering, The Pennsylvania State University, University Park, Pennsylvania 16802, USA.

The Review of Scientific Instruments
|July 2, 2009
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Summary

This study corrects the direct force balance method for atomic force microscopy lateral calibration. The improved method accounts for tip sliding on sloped surfaces, enhancing calibration accuracy.

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Area of Science:

  • Atomic Force Microscopy
  • Surface Science
  • Nanotechnology

Background:

  • The direct force balance method (DFBM) is used for lateral calibration in atomic force microscopy.
  • Previous DFBM assumed a pinned tip-substrate contact, neglecting sliding.
  • Tip sliding during force-distance measurements on sloped surfaces has been observed.

Purpose of the Study:

  • To report corrections and improvements to the direct force balance method (DFBM).
  • To address the assumption of pinned tip-substrate contact in the original DFBM.
  • To present an accurate force balance for lateral force calibration in atomic force microscopy.

Main Methods:

  • Utilizing lateral force signals from force-distance measurements on sloped surfaces.
  • Relating lateral force signals to applied load and surface slope.
  • Incorporating experimental observations of tip sliding during measurements.

Main Results:

  • Identified and corrected the assumption of pinned tip-substrate contact in DFBM.
  • Developed an improved force balance equation accounting for tip sliding.
  • Demonstrated enhanced accuracy in lateral calibration through corrected force balance.

Conclusions:

  • The previously reported DFBM required corrections due to unaddressed tip sliding.
  • The revised force balance provides a more accurate method for lateral calibration.
  • Accurate lateral calibration is crucial for reliable atomic force microscopy measurements.