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Reduction of titanium dioxide to metallic titanium conducted under the autogenic pressure of the reactants

Michal Eshed1, Alexander Irzh, Aharon Gedanken

  • 1Department of Chemistry, Kanbar Laboratory for Nanomaterials, Nanotechnology Research Center, Institute of Nanotechnology and Advanced Materials, Bar-Ilan University, Ramat-Gan 52900, Israel.

Inorganic Chemistry
|July 10, 2009
PubMed

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The radical dimerization of ketones or aldehydes gives vicinal diols through a pinacol coupling reaction. However, the behavior of titanium metals used for the reaction as a source of electrons is unusual. When the reaction is carried out in the presence of titanium, diols can be isolated at low temperatures. Else titanium further reacts with diols, forming alkenes through the McMurry reaction.