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Acoustic levitator for structure measurements on low temperature liquid droplets
J K R Weber1, C A Rey, J Neuefeind
1Materials Development, Inc., Arlington Heights, Illinois 60004, USA. info@matsdev.com
The Review of Scientific Instruments
|September 4, 2009
Summary
A novel acoustic levitator enables precise temperature control for studying supercooled liquids. This advanced setup allows for detailed structural investigations of liquids at sub-ambient temperatures.
Area of Science:
- Physics
- Materials Science
Background:
- Supercooled liquids are crucial for understanding glass transitions.
- Studying liquids at low temperatures presents significant experimental challenges.
Purpose of the Study:
- To develop and utilize a single-axis acoustic levitator for investigating the structure of supercooled liquids.
- To enable precise temperature control (-40 to +40 °C) of levitated samples.
Main Methods:
- Construction of a single-axis acoustic levitator with two 22 kHz acoustic transducers (up to 160 dB).
- Integration of a temperature-controlled gas flow system (Cryostream Plus) and infrared thermal imaging.
- Application of modulated acoustic forces to excite sample oscillations and investigation at the Advanced Photon Source (x-ray beamline 11 ID-C).
Main Results:
- Successful levitation of liquid and solid drops (1-3 mm diameter) within the specified temperature range.
- Demonstration of acoustic force modulation for exciting sample oscillations.
- Enabled in-situ structural investigation of supercooled liquids using X-ray scattering.
Conclusions:
- The developed acoustic levitator is a versatile tool for studying the properties of supercooled liquids.
- Precise temperature control and acoustic manipulation open new avenues for materials science research.
- The system facilitates advanced structural analysis of challenging liquid states.

