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Palladium N-Heterocyclic Carbene Complexes: Synthesis from Benzimidazolium Salts and Catalytic Activity in Carbon-carbon Bond-forming Reactions
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Microwave assisted synthesis, characterization and biological evaluation of palladium and platinum complexes with

Krishna Sharma1, Ritu Singh, Nighat Fahmi

  • 1Department of Chemistry, University of Rajasthan, Jaipur 302004, India.

Spectrochimica Acta. Part A, Molecular and Biomolecular Spectroscopy
|December 8, 2009
PubMed

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Direct alkylation of ammonia produces polyalkylated amines, along with a quaternary ammonium salt. To exclusively prepare primary amines, the azide synthesis method can be used.
Azide ions act as good nucleophiles and react with unhindered alkyl halides to form alkyl azides. Alkyl azides do not participate in further nucleophilic substitution reactions, thereby eliminating the chances of polyalkylated products. Alkyl azides are reduced by hydride-based reducing agents, like lithium aluminum...