Jove
Visualize
Contact Us
JoVE
x logofacebook logolinkedin logoyoutube logo
ABOUT JoVE
OverviewLeadershipBlogJoVE Help Center
AUTHORS
Publishing ProcessEditorial BoardScope & PoliciesPeer ReviewFAQSubmit
LIBRARIANS
TestimonialsSubscriptionsAccessResourcesLibrary Advisory BoardFAQ
RESEARCH
JoVE JournalMethods CollectionsJoVE Encyclopedia of ExperimentsArchive
EDUCATION
JoVE CoreJoVE BusinessJoVE Science EducationJoVE Lab ManualFaculty Resource CenterFaculty Site
Terms & Conditions of Use
Privacy Policy
Policies

Related Concept Videos

You might also read

Related Articles

Articles linked to this work by shared authors, journal, and citation graph.

Sort by
Same author

Mastering the potential of well-defined ML<sup>1</sup>L<sup>2</sup> species in asymmetric catalysis through ligand immobilization (ML<sup>het</sup>L<sup>hom</sup>). Use in highly enantioselective Pd-catalyzed spiroannulation.

Chemical science·2026
Same author

Automated Dynamic Flow Experimentation for Rapid Kinetic Fitting of Transition Metal Catalysis.

Angewandte Chemie (International ed. in English)·2026
Same author

Electrolysis-Assisted Reduction of Dimethylformamide for Unactivated Alkene Functionalizations.

Journal of the American Chemical Society·2026
Same author

Low Serum Lysophospholipids Predict Increased In-Hospital Mortality in Patients With Acute Heart Failure.

Journal of the American Heart Association·2026
Same author

Impact of Intended Isocaloric Early versus Late Time-Restricted Eating on Plasma Lipidome in Women with Overweight or Obesity: Secondary Analysis of the ChronoFast Trial.

Advanced science (Weinheim, Baden-Wurttemberg, Germany)·2025
Same author

Direct utilization of hydrogen sulfide gas for aryl thiol synthesis <i>via</i> adaptive dynamic homogeneous catalysis in a flow system.

Chemical communications (Cambridge, England)·2025

Related Experiment Video

Updated: Jun 18, 2026

Automated Modular High Throughput Exopolysaccharide Screening Platform Coupled with Highly Sensitive Carbohydrate Fingerprint Analysis
12:02

Automated Modular High Throughput Exopolysaccharide Screening Platform Coupled with Highly Sensitive Carbohydrate Fingerprint Analysis

Published on: April 11, 2016

Microwave-assisted high-throughput derivatization techniques utilizing silicon carbide microtiter platforms.

Markus Damm1, Gerald Rechberger, Manfred Kollroser

  • 1Christian Doppler Laboratory for Microwave Chemistry (CDLMC) and Institute of Chemistry, Karl-Franzens-University Graz, Heinrichstrasse 28, A-8010 Graz, Austria.

Journal of Chromatography. A
|December 8, 2009
PubMed
Summary

Parallel microwave-assisted derivatization using a silicon carbide platform significantly cuts analysis time for gas chromatography (GC) methods. This high-throughput approach enables rapid, simultaneous sample preparation for GC-Mass Spectrometry (GC-MS).

More Related Videos

A Microwave-Assisted Direct Heteroarylation of Ketones Using Transition Metal Catalysis
07:06

A Microwave-Assisted Direct Heteroarylation of Ketones Using Transition Metal Catalysis

Published on: February 16, 2020

Preparation of Silica Nanoparticles Through Microwave-assisted Acid-catalysis
09:43

Preparation of Silica Nanoparticles Through Microwave-assisted Acid-catalysis

Published on: December 16, 2013

Related Experiment Videos

Last Updated: Jun 18, 2026

Automated Modular High Throughput Exopolysaccharide Screening Platform Coupled with Highly Sensitive Carbohydrate Fingerprint Analysis
12:02

Automated Modular High Throughput Exopolysaccharide Screening Platform Coupled with Highly Sensitive Carbohydrate Fingerprint Analysis

Published on: April 11, 2016

A Microwave-Assisted Direct Heteroarylation of Ketones Using Transition Metal Catalysis
07:06

A Microwave-Assisted Direct Heteroarylation of Ketones Using Transition Metal Catalysis

Published on: February 16, 2020

Preparation of Silica Nanoparticles Through Microwave-assisted Acid-catalysis
09:43

Preparation of Silica Nanoparticles Through Microwave-assisted Acid-catalysis

Published on: December 16, 2013

Area of Science:

  • Analytical Chemistry
  • Chemical Engineering
  • Materials Science

Background:

  • Traditional gas chromatography (GC) derivatization is time-consuming.
  • High-throughput analytical methods are crucial for modern laboratories.

Purpose of the Study:

  • To develop parallel microwave-assisted derivatization protocols for enhanced GC analysis.
  • To evaluate a silicon carbide (SiC)-based platform for simultaneous sample preparation.

Main Methods:

  • Developed parallel microwave-assisted protocols for acetylation, pentafluoropropionylation, and trimethylsilylation.
  • Utilized a silicon carbide (SiC)-based microtiter plate platform with screw-capped GC vials.
  • Employed a multimode microwave instrument with online temperature monitoring for rapid, homogeneous heating.

Main Results:

  • Achieved complete derivatization for three standard protocols within 5 minutes at 100°C.
  • Demonstrated minimal temperature deviations across 80 simultaneous reaction mixtures on the SiC plate.
  • Confirmed comparable results using a standard hotplate, though with slightly slower heating.

Conclusions:

  • Parallel microwave derivatization significantly reduces overall analysis time.
  • The SiC platform enables high-throughput sample preparation under controlled conditions.
  • This method increases sample throughput for GC-MS-based analytical techniques.