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Related Concept Videos

X-ray Crystallography02:18

X-ray Crystallography

The size of the unit cell and the arrangement of atoms in a crystal may be determined from measurements of the diffraction of X-rays by the crystal, termed X-ray crystallography.
Diffraction
Diffraction is the change in the direction of travel experienced by an electromagnetic wave when it encounters a physical barrier whose dimensions are comparable to those of the wavelength of the light. X-rays are electromagnetic radiation with wavelengths about as long as the distance between neighboring...
Determination of Crystal Structures01:29

Determination of Crystal Structures

In the late 1800s, the revelation that light extended beyond visible wavelengths led to the discovery of X-rays by Wilhelm Roentgen. Recognized as high-energy electromagnetic radiation with short wavelengths, X-rays prompted exploration into their interaction with crystals. Max von Laue proposed in 1912 that the periodic arrangement of atoms, ions, or molecules in crystals would cause them to diffract X-rays, a hypothesis confirmed through experiments with copper sulfate and zinc sulfide...
X-ray Diffraction of Biological Samples01:10

X-ray Diffraction of Biological Samples

X-ray diffraction or XRD is an analytical tool that utilizes X-rays to study ordered structures such as crystalline organic and inorganic samples, polycrystalline materials, proteins, carbohydrates, and drugs.
According to Bragg's law, when X-rays strike the sample positioned on a stage, the rays are  scattered by the electron clouds around the sample atoms. The  X-ray diffraction or scattering is caused by constructive interference of the X-ray waves that reflect off the internal crystal...
Attenuated Total Reflectance (ATR) Infrared Spectroscopy: Overview01:13

Attenuated Total Reflectance (ATR) Infrared Spectroscopy: Overview

Attenuated total reflectance (ATR) infrared spectroscopy is a powerful analytical technique used to study the composition of materials. It is widely employed in chemistry, materials science, forensic science, and other fields where sample characterization is required. ATR has several advantages over traditional transmission IR spectroscopy, including the requirement of little to no sample preparation and the ability to analyze a wide range of samples.
The ATR process begins by directing a beam...

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Related Experiment Video

Updated: Jun 16, 2026

The Evolution of Silica Nanoparticle-polyester Coatings on Surfaces Exposed to Sunlight
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Published on: October 11, 2016

Reconstruction of surface profiles from their diffraction spectra.

J A Aas

    Applied Optics
    |February 2, 2010
    PubMed
    Summary

    This study presents a method to reconstruct 2D periodic surface profiles using diffraction spectra. The technique accurately reconstructs metal cylinder roughness, validated by laser measurements.

    Area of Science:

    • Optics and Photonics
    • Materials Science
    • Surface Metrology

    Background:

    • Characterizing surface topography is crucial for understanding material properties and performance.
    • Diffraction patterns contain rich information about surface structures.
    • Accurate reconstruction of surface profiles from optical measurements remains a challenge.

    Purpose of the Study:

    • To develop and demonstrate a method for reconstructing two-dimensional, periodic surface profiles from their diffraction spectra.
    • To validate the reconstruction method using experimental data.

    Main Methods:

    • Formulas for diffracted power distribution based on physical optics were summarized.
    • Real profiles were approximated by piecewise linear functions for computation.

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  • A steepest descent method was employed to reconstruct profiles from measured spectra.
  • A computer program iteratively optimized profiles to match measured spectra.
  • Main Results:

    • The study successfully reconstructed two-dimensional, periodic surface profiles.
    • Experimental validation using a CO(2) laser demonstrated the method's efficacy on a turned metal cylinder.
    • Reconstructed profiles were compared favorably with traditional tracing methods.

    Conclusions:

    • The developed method provides a viable approach for non-contact surface profile reconstruction from diffraction spectra.
    • This technique offers potential for precise surface metrology in various scientific and industrial applications.