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Related Concept Videos

Atomic Emission Spectroscopy: Lab01:29

Atomic Emission Spectroscopy: Lab

AES is a powerful analytical technique, especially effective when used with plasma sources, producing abundant spectra in characteristic emission lines. The Inductively Coupled Plasma (ICP), in particular, yields superior quantitative analytical data due to its high stability, low noise, low background, and minimal interferences under optimal experimental conditions. However, newer air-operated microwave sources are emerging as promising alternatives that could be more cost-effective than...
Standing Waves in a Cavity01:28

Standing Waves in a Cavity

A household microwave and lasers are examples of standing electromagnetic waves in a cavity. When two conducting metal plates are placed parallel at the nodal planes, it creates a cavity where standing waves are formed. The cavity between the two planes is analogous to a stretched string held at the points x = 0 and x = L. Here, the distance 'L' between the two planes must be an integer multiple of half of the wavelength. The wavelengths that satisfy this condition are given by:
Scanning Electron Microscopy01:07

Scanning Electron Microscopy

A scanning electron microscope (SEM) is used to study the surface features of a sample by using an electron beam that scans the sample surface in a two-dimensional manner. Typically, areas between ~1 centimeter to 5 micrometers in width can be imaged. SEM can be used to image bacteria, viruses, tissues as well as larger samples like insects. Conventional SEM gives a magnification ranging from 20X to 30,000X and spatial resolution of 50 to 100 nanometers.
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Interaction of EM Radiation with Matter: Spectroscopy01:12

Interaction of EM Radiation with Matter: Spectroscopy

Electromagnetic (EM) radiation can be considered an oscillating electric and magnetic field propagating through a medium that can interact with matter in its path. The electric field in the radiation can interact with electrical charges in the atoms or molecules in the matter. On the other hand, the magnetic field can interact with the magnetic field in the atomic nucleus. The study of the interaction between electromagnetic radiation and matter is termed spectroscopy. Spectroscopy is the study...
Atomic Emission Spectroscopy: Instrumentation01:22

Atomic Emission Spectroscopy: Instrumentation

The instrumentation of atomic emission spectrometry (AES) involves various components, including atomization devices that convert samples into gas-phase atoms and ions. There are two main types of atomization devices: continuous and discrete atomizers.  Continuous atomizers, like plasmas and flames, introduce samples in a constant stream, while discrete atomizers inject individual samples using syringes or autosamplers. The most common discrete atomizer is the electrothermal atomizer.

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Comprehensive Characterization of Extended Defects in Semiconductor Materials by a Scanning Electron Microscope
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Cavity methods for determining the emittance of solids.

E M Sparrow, P D Kruger, R P Heinisch

    Applied Optics
    |February 4, 2010
    PubMed
    Summary

    This study presents analytical results for radiation in cavities with nonisothermal walls, aiding experimental determination of solid material emittance. The findings enable simultaneous measurement of emittance and surface temperature.

    Area of Science:

    • Thermodynamics
    • Heat Transfer
    • Materials Science

    Background:

    • Experimental determination of solid emittance is crucial for thermal management.
    • Cavity-based methods are employed to mitigate surface condition effects.
    • Nonisothermal wall conditions in cavities present unique challenges for accurate emittance measurement.

    Purpose of the Study:

    • To develop analytical solutions for radiation heat transfer in cavities with nonisothermal walls.
    • To provide a framework for experimental determination of solid material emittance using cavity methods.
    • To enable simultaneous measurement of material emittance and surface temperature.

    Main Methods:

    • Solving coupled problems of radiative transport within the cavity.
    • Implementing two-dimensional heat conduction analysis in the bounding solid.

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  • Analyzing radiant flux from the cavity base as a function of emittance and cavity geometry.
  • Main Results:

    • Radiant flux results are presented as a function of emittance, depth-radius ratio, and temperature gradient parameter.
    • The study provides data to correlate cavity radiance measurements with material properties.
    • A method for simultaneous determination of emittance and exposed face temperature is described.

    Conclusions:

    • The analytical results facilitate accurate experimental determination of solid emittance.
    • The developed method allows for simultaneous measurement of emittance and surface temperature.
    • This work enhances the reliability of thermal property measurements in materials science.