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Recent trends in solid phase spectrometry: 2003-2009. A review.

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This review covers analytical methods for direct light measurement in solid phases, focusing on flow injection-solid phase spectrometry. This technique offers a simple, inexpensive, and potentially green approach for analyzing various compounds and metal ions.

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Area of Science:

  • Analytical Chemistry
  • Spectrometry

Background:

  • Direct light measurement of solid phases is crucial for analyzing concentrated analytes.
  • Flow injection-solid phase spectrometry (FI-SPS) has emerged as a key technique for routine analysis.

Purpose of the Study:

  • To review analytical methods for direct light measurement in solid phases.
  • To highlight the advancements and potential of flow injection-solid phase spectrometry.

Main Methods:

  • Review of approximately 100 papers published from 2003 to the present.
  • Focus on analytical methods involving direct light measurement of solid-phase concentrated analytes.
  • Examination of flow injection analysis (FIA) improvements like sequential injection and lab-on-a-valve.

Main Results:

  • FI-SPS is a simple, inexpensive tool for analyzing organic compounds and pharmaceuticals.
  • Advancements in FIA reduce reagent consumption and enable automated, miniaturized systems.
  • These developments align with green analytical chemistry principles.

Conclusions:

  • Flow injection-solid phase spectrometry is a promising technique for routine analysis.
  • Miniaturized and automated systems offer efficiency and reduced environmental impact.
  • Future applications include speciation of trace chemical components, such as metal ions in environmental samples.