Related Experiment Video

Updated: Jun 13, 2026

Crystallization and In Situ Room Temperature Data Collection Using the Crystallization Facility at Harwell and Beamline VMXi, Diamond Light Source
07:08

Crystallization and In Situ Room Temperature Data Collection Using the Crystallization Facility at Harwell and Beamline VMXi, Diamond Light Source

Published on: March 8, 2024

Measurements of mosaicity and perfection of crystallites in commercially available crystals using a 4-axis

F E Christensen, K P Singh, N J Westergaard

    Applied Optics
    |May 11, 2010
    PubMed

    More Related Videos

    Synchrotron X-ray Microdiffraction and Fluorescence Imaging of Mineral and Rock Samples10:12

    Synchrotron X-ray Microdiffraction and Fluorescence Imaging of Mineral and Rock Samples

    Published on: June 19, 2018

    High Pressure Single Crystal Diffraction at PX^211:32

    High Pressure Single Crystal Diffraction at PX^2

    Published on: January 16, 2017

    Related Concept Videos

    Determination of Crystal Structures01:29

    Determination of Crystal Structures

    In the late 1800s, the revelation that light extended beyond visible wavelengths led to the discovery of X-rays by Wilhelm Roentgen. Recognized as high-energy electromagnetic radiation with short wavelengths, X-rays prompted exploration into their interaction with crystals. Max von Laue proposed in 1912 that the periodic arrangement of atoms, ions, or molecules in crystals would cause them to diffract X-rays, a hypothesis confirmed through experiments with copper sulfate and zinc sulfide...
    X-ray Crystallography02:18

    X-ray Crystallography

    The size of the unit cell and the arrangement of atoms in a crystal may be determined from measurements of the diffraction of X-rays by the crystal, termed X-ray crystallography.
    Diffraction
    Diffraction is the change in the direction of travel experienced by an electromagnetic wave when it encounters a physical barrier whose dimensions are comparable to those of the wavelength of the light. X-rays are electromagnetic radiation with wavelengths about as long as the distance between neighboring...
    X-ray Diffraction of Biological Samples01:10

    X-ray Diffraction of Biological Samples

    X-ray diffraction or XRD is an analytical tool that utilizes X-rays to study ordered structures such as crystalline organic and inorganic samples, polycrystalline materials, proteins, carbohydrates, and drugs.
    According to Bragg's law, when X-rays strike the sample positioned on a stage, the rays are  scattered by the electron clouds around the sample atoms. The  X-ray diffraction or scattering is caused by constructive interference of the X-ray waves that reflect off the internal crystal...
    Imperfections in Crystal Structure: Point, Line and Plane Defects01:25

    Imperfections in Crystal Structure: Point, Line and Plane Defects

    A perfect crystal, in theory, has a uniform structure with the same unit cell and lattice points throughout. However, any deviation from this periodic arrangement is known as an imperfection or defect. These defects can be categorized into three types: point, line, and plane defects.Point defects occur when there is a deviation from the ideal due to missing atoms, displaced atoms, or additional atoms. These imperfections might occur due to imperfect packing during crystallization or because of...
    Imperfections in Crystal Structure: Stoichiometric Point Defects01:26

    Imperfections in Crystal Structure: Stoichiometric Point Defects

    Schottky defects arise when some lattice points in a crystal, such as those in NaCl, remain unoccupied, creating lattice vacancies without disturbing the overall electrical neutrality of the crystal. This defect is common in ionic crystals where the positive and negative ions are similar in size, as seen in sodium chloride and cesium chloride. The presence of Schottky defects enables the crystal to conduct electricity to a small extent through an ionic mechanism. Electric fields cause nearby...
    Imperfections in Crystal Structure: Non-Stoichiometric Defects01:29

    Imperfections in Crystal Structure: Non-Stoichiometric Defects

    Non-stoichiometric defects refer to a type of defect in the crystal structure of a compound where the ratio of its constituent elements deviates from the ideal stoichiometric ratio. There are two main types of non-stoichiometric defects: metal excess defects and metal deficiency defects.Metal excess defects occur when there is a slight surplus of metal ions than what is required by the stoichiometric ratio of the compound. For example, heating a sodium chloride crystal in sodium vapor results...