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Related Concept Videos

Inductively Coupled Plasma Atomic Emission Spectroscopy: Instrumentation01:26

Inductively Coupled Plasma Atomic Emission Spectroscopy: Instrumentation

Inductively coupled plasma (ICP) is the common plasma source used in atomic emission spectroscopy (AES), a technique that detects and analyzes various elements in a sample. This method is often called inductively coupled plasma atomic emission spectroscopy (ICP-AES).
There are three main types of inductively coupled plasma atomic emission spectroscopy  (ICP-AES) instruments: sequential, simultaneous multichannel, and Fourier transform instruments, with the latter being less commonly used.
Atomic Emission Spectroscopy: Instrumentation01:22

Atomic Emission Spectroscopy: Instrumentation

The instrumentation of atomic emission spectrometry (AES) involves various components, including atomization devices that convert samples into gas-phase atoms and ions. There are two main types of atomization devices: continuous and discrete atomizers.  Continuous atomizers, like plasmas and flames, introduce samples in a constant stream, while discrete atomizers inject individual samples using syringes or autosamplers. The most common discrete atomizer is the electrothermal atomizer.
Tandem Mass Spectrometry01:21

Tandem Mass Spectrometry

Tandem mass spectrometry is a technique that uses multiple mass analyzers in series to obtain a higher selectivity and reduce chemical noise during analyte detection. Instruments with multiple analyzers separated by an interaction cell enable secondary fragmentation and selected study of the fragment ions.Secondary fragmentations occur in the interaction cell and can be induced by various factors. Fragmentation induced by collision with inert gases, such as N2, Ar, He, etc., is called...
Atomic Absorption Spectroscopy: Instrumentation01:22

Atomic Absorption Spectroscopy: Instrumentation

An atomic absorption spectrophotometer (AAS) comprises several components: a radiation source, an atomizer, a monochromator, and a detector. The radiation source can be a hollow-cathode lamp (HCL) or an electrodeless-discharge lamp (EDL), both of which provide a narrow emission line of the required wavelength. However, some instruments use continuum sources and high-resolution monochromators to achieve a narrow range of radiation.
The atomizer used in AAS can be either a flame atomizer or an...
Electron Microscope Tomography and Single-particle Reconstruction01:07

Electron Microscope Tomography and Single-particle Reconstruction

Transmission electron microscopy (TEM) can be used to determine the 3D structure of biological samples with the help of techniques such as electron microscope tomography and single-particle reconstruction. While single-particle reconstruction can examine macromolecules and macromolecular complexes in vitro conditions only, tomography permits the study of cell components or small cells in vivo.
Electron Tomography
Electron tomography can be performed either in TEM or STEM (scanning transmission...
Atomic Emission Spectroscopy: Lab01:29

Atomic Emission Spectroscopy: Lab

AES is a powerful analytical technique, especially effective when used with plasma sources, producing abundant spectra in characteristic emission lines. The Inductively Coupled Plasma (ICP), in particular, yields superior quantitative analytical data due to its high stability, low noise, low background, and minimal interferences under optimal experimental conditions. However, newer air-operated microwave sources are emerging as promising alternatives that could be more cost-effective than...

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Related Experiment Video

Updated: Jun 11, 2026

Experimental Methods for Spin- and Angle-Resolved Photoemission Spectroscopy Combined with Polarization-Variable Laser
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Experimental Methods for Spin- and Angle-Resolved Photoemission Spectroscopy Combined with Polarization-Variable Laser

Published on: June 28, 2018

A rotatable electron spectrometer for multicoincidence experiments.

D Céolin1, J-O Forsell, B Wannberg

  • 1Department of Physics and Astronomy, Uppsala University, P.O. Box 516, SE-751 20 Uppsala, Sweden.

The Review of Scientific Instruments
|July 2, 2010
PubMed
Summary
This summary is machine-generated.

A new rotatable hemispherical spectrometer offers precise electron analysis and coincidence measurements. This advanced setup enhances experimental capabilities for studying particle interactions with high energy and angular resolution.

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Area of Science:

  • Atomic, Molecular, and Optical Physics
  • Surface Science
  • Quantum Chemistry

Background:

  • Characterizing electron emission requires sophisticated spectroscopic tools.
  • Existing spectrometers often have limitations in angular positioning and coincidence detection capabilities.
  • The need for versatile setups capable of multi-particle coincidence experiments is growing.

Purpose of the Study:

  • To develop and characterize a novel rotatable hemispherical spectrometer.
  • To enable high-resolution electron energy and angular distribution measurements.
  • To facilitate coincidence measurements between electrons and other particles (ions, photons).

Main Methods:

  • Designed a rotatable hemispherical analyzer with arbitrary lens axis positioning within a 1π solid angle.
  • Integrated a three-axes goniometer for precise control of electron collection angle relative to light polarization.
  • Employed a delay line detector and time-to-digital converter for electron impact position detection, replacing conventional CCD cameras.

Main Results:

  • Achieved good energy and angular resolution for electron spectroscopy.
  • Demonstrated the capability for positioning the spectrometer lens axis flexibly.
  • Verified the design's suitability for multi-particle coincidence experiments by optimizing resolving power and acceptance angle.

Conclusions:

  • The developed rotatable hemispherical spectrometer is a versatile tool for advanced electron spectroscopy.
  • Its design facilitates complex coincidence experiments, crucial for detailed investigations of atomic and molecular processes.
  • The use of a delay line detector offers an alternative to CCD cameras for precise electron event localization.