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Manganese Oxide Nanoparticle Synthesis by Thermal Decomposition of Manganese(II) Acetylacetonate
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Published on: June 18, 2020

Single-step synthesis of manganese oxide octahedral molecular sieves with large pore sizes

Hui Huang1, Chun-Hu Chen, Linping Xu

  • 1Department of Chemistry, University of Connecticut, 55 N. Eagleville Rd., Unit 3060, Storrs, CT 06269-3060, USA.

Chemical Communications (Cambridge, England)
|July 3, 2010
PubMed

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Activated manganese(IV) oxide can selectively oxidize allylic and benzylic alcohols via a radical intermediate mechanism. Primary allylic alcohols are oxidized to aldehydes, while secondary allylic alcohols yield ketones. The redox reaction of potassium permanganate with an Mn(II) salt such as manganese sulfate (under either alkaline or acidic conditions), followed by thorough drying, yields the oxidizing agent: activated MnO2. While MnO2 is insoluble in the solvents used for the reaction, the...