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Published on: June 14, 2024
Sonochemical syntheses and characterization of nano-structured three-dimensional lead(II) coordination polymer
Leila Aboutorabi1, Ali Morsali
1Department of Chemistry, Payame Noor University, Abhar, Zanjan, Islamic Republic of Iran.
Abstract:
Nano-structured three-dimensional lead(II) coordination polymer, [Pb(μ(6)-Fum)](n) (1); {Fum=Fumarate}, has been synthesized by sonochemical method and characterized by scanning electron microscopy, X-ray powder diffraction, elemental analyses and IR spectroscopy. Solvent effects on size and morphology of nano-structured compound 1 have been studied. Calcination of the nano-sized compound 1 at 600°C under air atmosphere yields PbO nanoparticles. The thermal stability of compound 1 both its bulk and nano-size has been studied by thermal gravimetric (TG) and differential thermal (DTA) analyses and compared each other.
