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Nanosecond x-ray Laue diffraction apparatus suitable for laser shock compression experiments.

Matthew Suggit1, Giles Kimminau, James Hawreliak

  • 1Department of Physics, Clarendon Laboratory, University of Oxford, Parks Road, Oxford OX1 3PU, United Kingdom. matthew.suggit@physics.ox.ac.uk

The Review of Scientific Instruments
|September 7, 2010
PubMed
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Researchers generated quasiwhite-light X-rays using laser-produced plasma for single-crystal Laue diffraction. This method enables rapid X-ray diffraction pattern capture from shocked and unshocked silicon crystals.

Area of Science:

  • Materials Science
  • Plasma Physics
  • Crystallography

Background:

  • Laue diffraction is a powerful technique for analyzing crystal structures.
  • Generating suitable X-ray sources for rapid, single-shot diffraction experiments presents a challenge.
  • Laser-produced plasmas offer a potential route to high-brightness X-ray sources.

Purpose of the Study:

  • To develop a quasiwhite-light X-ray source for Laue diffraction.
  • To demonstrate the capability of this source for single-shot diffraction from single crystals.
  • To investigate the structural changes in laser-shocked silicon crystals.

Main Methods:

  • Utilized nanosecond bursts of X-rays from a laser-produced plasma containing mid-Z elements.
  • Generated a quasiwhite-light X-ray spectrum with energies from 3 to over 10 keV.

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  • Performed single-shot nanosecond Laue diffraction on unshocked and laser-shocked silicon crystals.

    • Main Results:

    • Successfully produced a quasiwhite-light X-ray spectrum suitable for Laue diffraction.
    • Recorded bright, single-shot nanosecond diffraction patterns from single crystals.
    • Obtained diffraction patterns from both unshocked and shocked silicon, indicating the method's applicability to dynamic studies.

    Conclusions:

    • Laser-produced plasma X-rays provide a viable source for rapid Laue diffraction.
    • The developed technique is suitable for studying dynamic processes like laser-induced shock in crystals.
    • Single-shot diffraction captures structural information from transient states in materials.