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Related Concept Videos

Raman Spectroscopy Instrumentation: Overview01:26

Raman Spectroscopy Instrumentation: Overview

A conventional Raman spectrophotometer includes a laser source, a sample holding system, a wavelength selector, and a detector.
The monochromatic laser source, typically using visible or near-infrared radiation, generates a highly focused beam of light. This light interacts with the molecules of the sample, scattering some of the light. Liquid and gaseous samples are usually tested in ordinary glass capillaries, while solids can be analyzed as powders packed in capillaries or as potassium...
Two-Dimensional (2D) NMR: Overview01:12

Two-Dimensional (2D) NMR: Overview

The 1D NMR spectrum of large and complex molecules like natural products has complicated splitting patterns and overlapping signals, which can be easily interpreted using 2-dimensional (2D) NMR. Unlike 1D NMR, 2D NMR has two frequency axes that provide the coupling information between the nucleus A and nucleus B in a molecule. The process from which 2D spectra are obtained has four steps.
The first step is the preparation period, during which nucleus A is excited with a radiofrequency pulse.
Inductively Coupled Plasma Atomic Emission Spectroscopy: Instrumentation01:26

Inductively Coupled Plasma Atomic Emission Spectroscopy: Instrumentation

Inductively coupled plasma (ICP) is the common plasma source used in atomic emission spectroscopy (AES), a technique that detects and analyzes various elements in a sample. This method is often called inductively coupled plasma atomic emission spectroscopy (ICP-AES).
There are three main types of inductively coupled plasma atomic emission spectroscopy  (ICP-AES) instruments: sequential, simultaneous multichannel, and Fourier transform instruments, with the latter being less commonly used.
NMR Spectrometers: Radiofrequency Pulses and Pulse Sequences01:17

NMR Spectrometers: Radiofrequency Pulses and Pulse Sequences

A pulse is a short burst of radio waves distributed over a range of frequencies that simultaneously excites all the nuclei in the sample. Upon passing a radio frequency pulse along the x-axis, the nuclei absorb energy corresponding to their Larmor frequencies and achieve resonance. This shifts the net magnetization vector from the z-axis toward the transverse plane. This angle of rotation of the magnetization vector, or the flip angle, is proportional to the duration and intensity of the pulse.
NMR Spectrometers: Overview01:20

NMR Spectrometers: Overview

NMR spectrometers consist of a strong magnet, a radiofrequency transmitter, and a detector attached to a computer console for recording spectra of samples containing NMR-active nuclei. In first-generation NMR instruments called continuous-wave spectrometers, the resonance frequencies of the nuclei are determined by frequency-sweep or field-sweep methods. The magnetic field strength is fixed and the rf signal is swept in the former, while the radiofrequency signal is fixed and the magnetic field...

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Related Experiment Video

Updated: Jun 8, 2026

Characterizing Far-infrared Laser Emissions and the Measurement of Their Frequencies
09:38

Characterizing Far-infrared Laser Emissions and the Measurement of Their Frequencies

Published on: December 18, 2015

Simultaneous line center and linewidth measurement using dual frequency modulation spectroscopy.

Jonathon I Gillen1, David H McIntyre

  • 1MIT–Harvard Center for Ultracold Atoms, Research Laboratory of Electronics, and Department of Physics, Massachusetts Institute of Technology, Cambridge Massachusetts 02139, USA.

Applied Optics
|October 12, 2010
PubMed
Summary

This study introduces a novel dual frequency modulation technique to precisely measure spectral feature center frequency and linewidth simultaneously. This method enables accurate frequency control for spectroscopic applications.

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Area of Science:

  • Spectroscopy
  • Optical Physics
  • Metrology

Background:

  • Precise characterization of spectral features is crucial for various scientific and technological applications.
  • Existing methods often require separate measurements for center frequency and linewidth, increasing complexity and time.

Purpose of the Study:

  • To develop a single, simultaneous measurement technique for both the center frequency and frequency linewidth of spectral features.
  • To enable robust frequency control of laser systems based on spectral feature properties.

Main Methods:

  • Utilizing dual frequency modulation of a carrier frequency to probe spectral features.
  • Employing phase-sensitive detection at the two modulation frequencies to analyze the transmitted signal.
  • Implementing servo-stabilization loops for precise frequency control of the carrier and modulation frequencies.

Main Results:

  • Successfully demonstrated simultaneous measurement of spectral feature center frequency and frequency linewidth.
  • Developed a method for servo-stabilizing the carrier frequency to the resonance line center.
  • Achieved servo-stabilization of one modulation frequency to the resonance linewidth.

Conclusions:

  • The proposed dual frequency modulation method offers an efficient and accurate approach for simultaneous spectral characterization.
  • This technique provides a foundation for advanced frequency control systems in spectroscopy and related fields.