Related Experiment Video
Updated: Jun 5, 2026

Preparation of Enantiopure Non-Activated Aziridines and Synthesis of Biemamide B, D, and epiallo-Isomuscarine
Published on: June 13, 2022
3-(3-Chloro-prop-yl)-7,8-dimeth-oxy-1H-3-benzazepin-2(3H)-one at 125 K
1Zhejiang Police College Experience Center, Zhejiang Police College, Hangzhou 310053, People's Republic of China.
Abstract:
In the title compound, C(15)H(18)ClNO(3), the seven-membered ring has a mirror plane passing through the methyl-ene C atom and bis-ecting the C=C bond. It adopts a bent conformation, inter-mediate between the boat and chair forms. Both meth-oxy groups are coplanar with the attached benzene ring [C-C-O-C = -0.5 (3) and 2.2 (3)°]. In the crystal structure, inversion-related mol-ecules are linked via C-H⋯O hydrogen bonds and π-π inter-actions involving the benzene ring [centroid-centroid distance = 3.6393 (12)Å].
More Related Videos
11:45Preparation of Stable Bicyclic Aziridinium Ions and Their Ring-Opening for the Synthesis of Azaheterocycles
Published on: August 22, 2018
14:11Synthesis of pH Dependent Pyrazole, Imidazole, and Isoindolone Dipyrrinone Fluorophores using a Claisen-Schmidt Condensation Approach
Published on: June 10, 2021