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19:58
Palladium N-Heterocyclic Carbene Complexes: Synthesis from Benzimidazolium Salts and Catalytic Activity in Carbon-carbon Bond-forming Reactions
Published on: July 30, 2017
Bis(4-pyridylmeth-yl) hexa-nedioate
Acta Crystallographica. Section E, Structure Reports Online
|January 5, 2011
Summary
This study details the crystal structure of a C18H20N2O4 compound. Weak hydrogen bonds form an intricate three-dimensional molecular network.
Area of Science:
- Crystallography
- Chemical Structure Analysis
Background:
- Understanding molecular structure is crucial in chemistry.
- Crystallography provides detailed insights into solid-state molecular arrangements.
Purpose of the Study:
- To elucidate the crystal structure of the title compound, C18H20N2O4.
- To analyze the molecular geometry and intermolecular interactions.
Main Methods:
- Single-crystal X-ray diffraction was employed.
- The crystal structure was solved and refined.
Main Results:
- The asymmetric unit contains one half-molecule, located on an inversion center.
- The molecule is nearly planar with slight twists between pyridine rings (torsion angles 170.9–177.2°).
- Weak C-H⋯O hydrogen bonds facilitate the formation of a 3D network.
Conclusions:
- The study provides a detailed structural characterization of C18H20N2O4.
- The observed hydrogen bonding network influences the compound's solid-state architecture.
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