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|January 5, 2011

Summary

This summary is machine-generated.

This study details the crystal structure of a C(14)H(16)N(2)O(2) compound, revealing its molecular conformation and stabilizing hydrogen bonds. The findings contribute to understanding molecular arrangements in crystalline solids.

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Area of Science:

Crystallography
Molecular Chemistry
Solid-State Chemistry

Background:

Understanding the precise three-dimensional arrangement of atoms within a molecule is crucial for predicting its properties and reactivity.
Crystal structure analysis provides fundamental insights into intermolecular interactions and solid-state behavior.

Purpose of the Study:

To determine and describe the crystal structure of the title compound, C(14)H(16)N(2)O(2).
To analyze the molecular conformation and identify the types of intermolecular interactions present in the crystal lattice.

Main Methods:

Single-crystal X-ray diffraction was employed to collect diffraction data.
The crystal structure was solved and refined using standard crystallographic software.

Main Results:

The molecule of C(14)H(16)N(2)O(2) lies on a crystallographic twofold rotation axis.
The central O-C-C-O bridge exhibits a gauche conformation.
One amine hydrogen atom is disordered over two equally probable sites.
The crystal structure is stabilized by a network of N-H⋯O and N-H⋯N hydrogen bonds.

Conclusions:

The detailed crystal structure of C(14)H(16)N(2)O(2) has been elucidated.
The observed molecular conformation and hydrogen bonding patterns provide insights into the packing and stability of the compound in the solid state.