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Updated: Jun 5, 2026
![Microwave-assisted One-pot Synthesis of N-succinimidyl-4-[18F]fluorobenzoate ([18F]SFB)](/_next/image?url=https%3A%2F%2Fcloudfront.jove.com%2FCDNSource%2Fteasers%2F2755.jpg&w=3840&q=50)
Microwave-assisted One-pot Synthesis of N-succinimidyl-4-[18F]fluorobenzoate ([18F]SFB)
Published on: June 28, 2011
S-Benzyl-thio-uronium 3-nitro-benzene-sulfonate
Abstract:
In the title compound, C(8)H(11)N(2)S(+)·C(6)H(4)NO(5)S(-), the asymmetric unit is composed of two crystallographically independent S-benzyl-thio-uronium cations and two independent nitro-benzene-sulfonate anions. An intra-molecular hydrogen bond generates an S(5)S(5) ring motif. The crystal packing is stabilized by intra-molecular C-H⋯O and inter-molecular C-H⋯O, N-H⋯O and N-H⋯S hydrogen bonds which, along with short S⋯O [3.034 (2) Å] and N⋯O [2.796 (3) Å] contacts, form a two-dimensional network parallel to the ab plane.
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