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Updated: Jun 4, 2026

Synchrotron X-ray Microdiffraction and Fluorescence Imaging of Mineral and Rock Samples
Published on: June 19, 2018
The New NIST/ARPA National Soft X-Ray Reflectometry Facility
C Tarrio1, R N Watts, T B Lucatorto
1Physics Laboratory, National Institute of Standards and Technology, Gaithersburg, Maryland 20899.
Upgrades to the National Reflectometry Facility enhance its capabilities for measuring optical components. New equipment offers improved throughput and resolution for advanced lithography and astronomy applications.
Area of Science:
- Optical physics
- Synchrotron radiation applications
- Materials science instrumentation
Background:
- The NIST/ARPA National Reflectometry Facility is undergoing significant upgrades.
- Current capabilities are limited to measuring optical components smaller than 10 cm.
Purpose of the Study:
- To detail recent upgrades to the NIST/ARPA National Reflectometry Facility.
- To introduce a new monochromator and an upcoming larger sample manipulator.
- To present preliminary performance data for the new monochromator.
Main Methods:
- Installation of a new high-throughput monochromator.
- Utilizing an existing sample manipulator for smaller optics (<10 cm).
- Planning for a future manipulator for larger optics.
Main Results:
- The new monochromator provides high throughput and modest resolution.
- Wavelength range of the monochromator is 3.5-40 nm.
- Preliminary measurements confirm the performance characteristics.
Conclusions:
- The upgraded facility will support advanced scientific and technological endeavors.
- Future installations will expand the facility's capacity for larger optics.
- The new monochromator represents a key improvement in reflectometry capabilities.
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