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Synthesis of graphene oxide-based biocomposites through diimide-activated amidation

Jianfeng Shen1, Bo Yan, Min Shi

  • 1Center of Special Materials and Technology, Fudan University, Shanghai, China.

Journal of Colloid and Interface Science
|February 19, 2011
PubMed

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Preparation of Amides01:29

Preparation of Amides

Amides are synthesized by treating carboxylic acids with amines in the presence of dehydrating agents like dicyclohexylcarbodiimide (DCC).
The DCC-promoted synthesis of amides begins with the protonation of DCC by carboxylic acid. The protonation makes it a better acceptor. Next, the addition of carboxylate to the protonated carbodiimide gives a reactive acylating agent.
Subsequently, the amine acts as a nucleophile that attacks the acylating agent to form a tetrahedral intermediate. In the...