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Quantitative atom column position analysis at the incommensurate interfaces of a (PbS)(1.14)NbS(2) misfit layered

M Garbrecht1, E Spiecker, K Tillmann

  • 1Microanalysis of Materials, Institute of Materials Science, University of Kiel, 24143 Kiel, Germany. mag@technion.ac.il

Ultramicroscopy
|February 22, 2011
PubMed

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¹H NMR: Complex Splitting01:13

¹H NMR: Complex Splitting

A proton M that is coupled to a proton X results in doublet signals for M. However, NMR-active nuclei can be simultaneously coupled to more than one nonequivalent nucleus. When M is coupled to a second proton A, such as in styrene oxide, each peak in the doublet is split into another doublet.
Splitting diagrams or splitting tree diagrams are routinely used to depict such complex couplings. While drawing splitting diagrams, the splitting with the larger coupling constant is usually applied first.