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{6,6'-Dimeth-oxy-2,2'-[ethane-1,2-diylbis(nitrilo-methanylyl-idene)]diphenolato}nickel(II) dimethyl-formamide

Kouassi Ayikoé1, Ray J Butcher, Yilma Gultneh

  • 1Department of Chemistry, Howard University, 525 College Street NW, Washington, DC 20059, USA.

Acta Crystallographica. Section E, Structure Reports Online
|April 28, 2011
PubMed

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Precipitation Gravimetry

Precipitation gravimetry is based on converting an analyte into a sparingly soluble precipitate, which is separated by filtration and weighed. An ideal precipitate should be pure, insoluble, of known composition, and easily filtered from the reaction mixture.
In determining nickel by gravimetric analysis, a precipitant of ethanolic dimethylglyoxime is added to a hot nickel salt solution. This is quickly followed by the dropwise addition of dilute ammonia solution until precipitation occurs. A...