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Summary
This summary is machine-generated.

The crystal structure of C(8)H(5)FO(4) reveals a nearly planar molecule. Intermolecular interactions form a 2D supramolecular network, showcasing unique hydrogen bonding and C-H⋯F interactions.

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Area of Science:

  • Crystallography
  • Molecular structure
  • Supramolecular chemistry

Background:

  • Understanding molecular arrangements is crucial in materials science.
  • Crystal engineering utilizes intermolecular forces to design novel structures.
  • Fluorinated organic compounds exhibit unique chemical properties.

Purpose of the Study:

  • To elucidate the crystal structure of C(8)H(5)FO(4).
  • To investigate the intermolecular interactions governing the crystal packing.
  • To analyze the molecular planarity and symmetry.

Main Methods:

  • Single-crystal X-ray diffraction was employed to determine the atomic arrangement.
  • Symmetry analysis identified crystallographic twofold symmetry.
  • Dihedral angles were calculated to assess molecular planarity.
  • Intermolecular interactions (hydrogen bonds, C-H⋯F) were analyzed.

Main Results:

  • The crystal structure of C(8)H(5)FO(4) was determined.
  • The molecule exhibits approximate planarity with a dihedral angle of 2.01° between the carboxyl group and the benzene ring.
  • A two-dimensional supramolecular array is formed through O-H⋯O hydrogen bonds and C-H⋯F interactions.
  • Crystallographic twofold symmetry generates the complete molecular unit.

Conclusions:

  • The study provides detailed insights into the crystal packing of C(8)H(5)FO(4).
  • The observed intermolecular interactions dictate the formation of a 2D supramolecular network.
  • The findings contribute to the understanding of structure-property relationships in fluorinated organic compounds.