Related Experiment Video

Updated: Jun 2, 2026

Green Synthesis of Quinoline-Based Ionic Liquid
05:59

Green Synthesis of Quinoline-Based Ionic Liquid

Published on: September 27, 2024

Dimethyl 2-methyl-1,2-dihydro-quinoline-2,4-dicarboxyl-ate

Zeynep Gültekin, Wolfgang Frey, Barış Tercan

    Acta Crystallographica. Section E, Structure Reports Online
    |April 28, 2011
    PubMed

    Abstract:

    In the crystal of the title compound, C(14)H(15)NO(4), pairs of inter-molecular N-H⋯O hydrogen bonds link the mol-ecules into centrosymmetric R(2) (2)(10) dimers. These dimers are further connected via inter-molecular C-H⋯O hydrogen bonds, forming a three-dimensional network. The heterocyclic ring adopts a twisted conformation.

    More Related Videos

    Preparation of Enantiopure Non-Activated Aziridines and Synthesis of Biemamide B, D, and epiallo-Isomuscarine
    11:04

    Preparation of Enantiopure Non-Activated Aziridines and Synthesis of Biemamide B, D, and epiallo-Isomuscarine

    Published on: June 13, 2022

    Efficient Construction of Drug-like Bispirocyclic Scaffolds Via Organocatalytic Cycloadditions of α-Imino γ-Lactones and Alkylidene Pyrazolones
    10:17

    Efficient Construction of Drug-like Bispirocyclic Scaffolds Via Organocatalytic Cycloadditions of α-Imino γ-Lactones and Alkylidene Pyrazolones

    Published on: February 7, 2019

    Related Experiment Videos

    Last Updated: Jun 2, 2026

    Green Synthesis of Quinoline-Based Ionic Liquid
    05:59

    Green Synthesis of Quinoline-Based Ionic Liquid

    Published on: September 27, 2024

    Preparation of Enantiopure Non-Activated Aziridines and Synthesis of Biemamide B, D, and epiallo-Isomuscarine
    11:04

    Preparation of Enantiopure Non-Activated Aziridines and Synthesis of Biemamide B, D, and epiallo-Isomuscarine

    Published on: June 13, 2022

    Efficient Construction of Drug-like Bispirocyclic Scaffolds Via Organocatalytic Cycloadditions of α-Imino γ-Lactones and Alkylidene Pyrazolones
    10:17

    Efficient Construction of Drug-like Bispirocyclic Scaffolds Via Organocatalytic Cycloadditions of α-Imino γ-Lactones and Alkylidene Pyrazolones

    Published on: February 7, 2019

    Related Concept Videos

    Carboxylic Acids to Methylesters: Alkylation using Diazomethane01:33

    Carboxylic Acids to Methylesters: Alkylation using Diazomethane

    Carboxylic acids react with diazomethane in an ether solvent via alkylation at the carboxylate oxygen atom to give methyl esters of the corresponding acid with excellent yields.
    Loss of Carboxy Group as CO2: Decarboxylation of Malonic Acid Derivatives01:35

    Loss of Carboxy Group as CO2: Decarboxylation of Malonic Acid Derivatives

    Just like β-keto acids—which upon thermal decarboxylation form ketones—β-dicarboxylic acids undergo decarboxylation to generate monocarboxylic acids with the liberation of carbon dioxide.
    Alkylation of β-Diester Enolates: Malonic Ester Synthesis01:14

    Alkylation of β-Diester Enolates: Malonic Ester Synthesis

    Malonic ester synthesis is a method to obtain α substituted carboxylic acids from ꞵ-diesters such as diethyl malonate and alkyl halides.

    Articles linked to this work by shared authors, journal, and citation graph.

    Synthesis and structure of 9-(di-methyl-amino)-1,10-phenanthrolin-1-ium nitrate.

    Acta crystallographica. Section E, Crystallographic communications·2026

    Synthesis, structure and energy calculations of 4-{4-[(2,3-dioxoindol-1-yl)meth-yl]-1H-1,2,3-triazol-1-yl}butyl acetate.

    Acta crystallographica. Section E, Crystallographic communications·2026

    Synthesis, crystal structure and Hirshfeld surface analysis of 1-(3,4-di-chloro-phen-yl)-4,4,6-trimethyl-3,4-di-hydro-pyrimidine-2(1H)-thione.

    Acta crystallographica. Section E, Crystallographic communications·2026

    Synthesis and structure of 5,5'-(tris-ulfane-1,3-di-yl)bis-(1,3,4-thia-diazol-2-amine).

    Acta crystallographica. Section E, Crystallographic communications·2026

    Synthesis, crystal structure determination, Hirshfeld surface and crystal void analyses, inter-action energy calculations and energy frameworks of N-(2-chloro-phen-yl)-N'-propano-ylthio-urea.

    Acta crystallographica. Section E, Crystallographic communications·2026

    Crystal structure and Hirshfeld surface analyses, inter-action energy calculations and energy frameworks of (Z)-4-benzyl-2-(4-methyl-benzylidene)-2H-[1,4]benzo-thia-zin-3(4H)-one.

    Acta crystallographica. Section E, Crystallographic communications·2026

    Crystal structure of 1-(piperidin-1-yl)butane-1,3-dione.

    Acta crystallographica. Section E, Structure reports online·2015

    Crystal structure of methyl 1-methyl-3,5-diphenyl-7-tosyl-3,6,7,11b-tetra-hydro-pyrazolo-[4',3':5,6]pyrano[3,4-c]quinoline-5a(5H)-carboxyl-ate.

    Acta crystallographica. Section E, Structure reports online·2015

    Crystal structure of 4-amino-1-(4-methyl-benz-yl)pyridinium bromide.

    Acta crystallographica. Section E, Structure reports online·2015

    Crystal structure of (Z)-3-benz-yloxy-6-[(2-hy-droxy-anilino)methyl-idene]cyclo-hexa-2,4-dien-1-one.

    Acta crystallographica. Section E, Structure reports online·2015

    Crystal structure of bis-(1-benzyl-1H-1,2,4-triazole) perchloric acid monosolvate.

    Acta crystallographica. Section E, Structure reports online·2015

    Crystal structure of 2-(di-phenyl-phos-phanyl)phenyl 4-(hy-droxy-meth-yl)benzoate.

    Acta crystallographica. Section E, Structure reports online·2015

    Astragaloside IV Protects against PM2.5-Induced Spermatocyte Injury via the cGAS-STING/Nrf2/HMOX1 Axis.

    Reproductive toxicology (Elmsford, N.Y.)·2026

    Alleviation of senkyunolide A on hyperuricemia and hyperuricemia-induced renal damage in rats.

    Biochemical and biophysical research communications·2026

    Pharmacological investigation of a selected triazole derivative against acetic acid-induced ulcerative colitis in mouse model.

    Biochemical and biophysical research communications·2026

    Integrated experimental and computational investigation of sophoridine derivatives reveals antitumor potential and Topo I-associated mechanisms.

    European journal of medicinal chemistry·2026

    Discovery of Aspxanthones A-I with SIRT1 agonist activity from Aspergillus sp. TJ507.

    Bioorganic chemistry·2026

    Benzo[h]quinoline-based heterocyclic derivatives as Culex pipiens larvicidal candidates: synthesis, bioactivity, biochemical response, and in silico mechanistic insights.

    Bioorganic chemistry·2026
    See all related articles
    JoVE
    x logofacebook logolinkedin logoyoutube logo
    ABOUT JoVE
    OverviewLeadershipBlogJoVE Help Center
    AUTHORS
    Publishing ProcessEditorial BoardScope & PoliciesPeer ReviewFAQSubmit
    LIBRARIANS
    TestimonialsSubscriptionsAccessResourcesLibrary Advisory BoardFAQ
    RESEARCH
    JoVE JournalMethods CollectionsJoVE Encyclopedia of ExperimentsArchive
    EDUCATION
    JoVE CoreJoVE BusinessJoVE Science EducationJoVE Lab ManualFaculty Resource CenterFaculty Site
    Terms & Conditions of Use
    Privacy Policy
    Policies
    Jove
    Visualize
    Contact Us