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4-(2-Chloro-ethyl)morpholinium picrate.

Rajni Kant, Sabeta Kohli, Lovely Sarmal

    Acta Crystallographica. Section E, Structure Reports Online
    |May 18, 2011
    PubMed
    Summary
    This summary is machine-generated.

    A novel salt, C(6)H(13)ClNO(+)·C(6)H(2)N(3)O(7) (-), was synthesized using picric acid and 4-(2-chloro-ethyl)morpholine. Its crystal structure is stabilized by hydrogen bonds.

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    Area of Science:

    • Crystallography
    • Organic Chemistry
    • Chemical Synthesis

    Background:

    • Picric acid is a well-known explosive and reagent.
    • Morpholine derivatives are widely used in various chemical applications.
    • Understanding the structural properties of novel compounds is crucial for material science.

    Purpose of the Study:

    • To synthesize and characterize a new salt formed from picric acid and 4-(2-chloro-ethyl)morpholine.
    • To elucidate the crystal structure of the synthesized compound.
    • To identify the intermolecular interactions stabilizing the crystal lattice.

    Main Methods:

    • Chemical synthesis involving the reaction of picric acid with 4-(2-chloro-ethyl)morpholine.
    • Single-crystal X-ray diffraction to determine the molecular and crystal structure.
    • Analysis of hydrogen bonding interactions (C-H⋯O and N-H⋯O).

    Main Results:

    • Successful synthesis of the title compound, C(6)H(13)ClNO(+)·C(6)H(2)N(3)O(7) (-).
    • Determination of the crystal structure, revealing the arrangement of the cation and anion.
    • Identification of significant C-H⋯O and N-H⋯O hydrogen bonds contributing to crystal stability.

    Conclusions:

    • The synthesis yielded a novel salt with potential applications in chemical research.
    • The crystal structure analysis provides insights into the supramolecular assembly driven by hydrogen bonding.
    • The findings contribute to the understanding of structure-property relationships in organic salts.