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Solid-state Graft Copolymer Electrolytes for Lithium Battery Applications
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Lithium samarium polyphosphate, LiSm(PO(3))(4).

Dan Zhao, Feifei Li, Wendan Cheng

    Acta Crystallographica. Section E, Structure Reports Online
    |May 18, 2011
    PubMed
    Summary

    Researchers characterized LiSm(PO(3))(4), a mixed-metal rare-earth polyphosphate. This compound features a 3D framework built from zigzag phosphate chains linked by lithium and samarium ions.

    Area of Science:

    • Materials Science
    • Inorganic Chemistry
    • Solid-State Chemistry

    Background:

    • Rare-earth polyphosphates are an important class of inorganic compounds.
    • Mixed-metal polyphosphates offer tunable properties for various applications.

    Purpose of the Study:

    • To synthesize and characterize the novel mixed-metal rare-earth polyphosphate, LiSm(PO(3))(4).
    • To elucidate the crystal structure and bonding characteristics of LiSm(PO(3))(4).

    Main Methods:

    • Single-crystal X-ray diffraction was employed to determine the crystal structure.
    • Chemical analysis confirmed the stoichiometry of the compound.

    Main Results:

    • LiSm(PO(3))(4) crystallizes in a three-dimensional framework structure.

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  • The framework consists of zigzag polyphosphate chains [(PO(3))(n)](n-) linked by Li(+) and Sm(3+) cations.
  • Both Li(+) and Sm(3+) ions occupy sites with 2. symmetry.

    • Conclusions:

    • The study successfully synthesized and characterized LiSm(PO(3))(4).
    • The unique 3D framework structure highlights the potential of mixed-metal rare-earth polyphosphates in materials science.