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Related Experiment Video

Updated: Jun 1, 2026

Nucleoside Triphosphates - From Synthesis to Biochemical Characterization
15:22

Nucleoside Triphosphates - From Synthesis to Biochemical Characterization

Published on: April 3, 2014

N-(6-Methyl-2-pyrid-yl)formamide.

Hui-Ling Hu, Chia-Jun Wu, Pei-Chi Cheng

    Acta Crystallographica. Section E, Structure Reports Online
    |May 18, 2011
    PubMed
    Summary

    The crystal structure of C(7)H(8)N(2)O reveals a nearly planar molecule. Self-complementary amide groups form hydrogen bonds, creating centrosymmetric dimers in the crystal lattice.

    Area of Science:

    • Crystallography
    • Molecular structure analysis

    Background:

    • Understanding the three-dimensional arrangement of atoms in molecules is crucial for predicting chemical properties and reactivity.
    • Crystal engineering utilizes intermolecular interactions to design and construct materials with desired properties.

    Purpose of the Study:

    • To determine the precise molecular geometry and crystal packing of the title compound, C(7)H(8)N(2)O.
    • To investigate the role of hydrogen bonding in the self-assembly of molecules in the solid state.

    Main Methods:

    • Single-crystal X-ray diffraction was employed to collect diffraction data.
    • The crystal structure was solved and refined using standard crystallographic software.

    Main Results:

    • The molecule C(7)H(8)N(2)O was found to be essentially planar, with a maximum atomic deviation of 0.0439(1) Å from the least-squares plane.

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  • Intermolecular N-H⋯O hydrogen bonds were observed between amide groups, leading to the formation of centrosymmetric dimers.
  • These dimers are the primary building blocks in the crystal structure.

    • Conclusions:

    • The planarity of the molecule influences its packing in the crystal lattice.
    • Hydrogen bonding plays a significant role in the formation of supramolecular structures in the solid state.
    • The observed dimer formation is a common motif in compounds containing amide functionalities.