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Updated: Jun 1, 2026

X-ray Powder Diffraction in Conservation Science: Towards Routine Crystal Structure Determination of Corrosion Products on Heritage Art Objects
Published on: June 8, 2016
Alaptide from synchrotron powder diffraction data
Abstract:
THE TITLE COMPOUND [SYSTEMATIC NAME: (8S)-8-methyl-6,9-diaza-spiro-[4.5]decane-7,10-dione], C(9)H(14)N(2)O(2), consists of two connected rings, viz. a piperazine-2,5-dione (DKP) ring and a five-membered ring. The DKP ring adopts a slight boat conformation and the bonded methyl group is in an equatorial position. The five-membered ring is in an envelope conformation. In the crystal structure, inter-molecular N-H⋯O hydrogen bonds link mol-ecules into chains running parallel to the c axis.
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