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Updated: Jun 1, 2026
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Solid-phase Synthesis of [4.4] Spirocyclic Oximes
Published on: February 6, 2019
4-Benz-yloxy-3-(2,4-dichloro-phen-yl)-1-oxaspiro-[4.5]dec-3-en-2-one
Liang-Zhong Xu1, Qun-Qun Su, Jin Huang
1College of Chemistry and Molecular Engineering, Qingdao University of Science and Technology, Qingdao 266042, People's Republic of China.
Abstract:
In the title compound, C(22)H(20)Cl(2)O(3), the cyclo-hexyl ring adopts a chair conformation. The furanyl ring plane makes dihedral angles of 70.10 (2) and 86.12 (3)° with the 2,4-dichloro-phenyl ring and aromatic ring of the benzyl group, respectively. The crystal structure features weak inter-molecular C-H⋯O and C-H⋯Cl hydrogen bonds.
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