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Dimorpholinium penta-chloridoanti-monate(III).

Li Zhuang Chen1

  • 1Ordered Matter Science Research Center, College of Chemistry and Chemical Engineering, Southeast University, Nanjing 210096, People's Republic of China.

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Summary

This study details the crystal structure of a morpholinium compound containing antimony pentachloride. It highlights hydrogen bonding interactions between morpholinium cations and the antimony-based anion.

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Area of Science:

  • Inorganic Chemistry
  • Crystallography
  • Structural Chemistry

Background:

  • Morpholinium salts are organic compounds with diverse applications.
  • Antimony pentachloride is a key inorganic compound with various coordination geometries.
  • Understanding hydrogen bonding in ionic compounds is crucial for predicting material properties.

Purpose of the Study:

  • To elucidate the crystal structure of the morpholinium antimony pentachloride compound.
  • To characterize the coordination environment of the antimony ion.
  • To investigate the hydrogen bonding network within the crystal lattice.

Main Methods:

  • Single-crystal X-ray diffraction was employed to determine the molecular and crystal structure.
  • Analysis of intermolecular interactions, including hydrogen bonds, was performed.
  • Coordination geometry around the central antimony atom was analyzed.

Main Results:

  • The asymmetric unit contains two morpholinium cations and one penta-chloridoanti-monate dianion.
  • Morpholinium cations adopt chair conformations.
  • The antimony(III) ion exhibits a slightly distorted square-pyramidal coordination environment.
  • Hydrogen bonds of N-H⋯O and N-H⋯Cl types were identified, linking cations and anions.

Conclusions:

  • The crystal structure reveals a well-defined arrangement of morpholinium cations and penta-chloridoanti-monate anions.
  • Hydrogen bonding plays a significant role in stabilizing the crystal structure.
  • The findings contribute to the understanding of structural diversity in antimony-containing ionic compounds.