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Updated: Jun 1, 2026

High-resolution Tandem Mass Spectrometry for Studying Chemical Constituents of Gynura bicolor DC
Published on: February 2, 2024
7,7',8,8'-Tetra-meth-oxy-4,4'-dimethyl-3,3'-bicoumarin
Abstract:
In the crystal structure, the title compound, C(24)H(22)O(8), lies on a twofold rotation axis and the asymmetric unit comprises one half-mol-ecule. The dihedral angle formed by the coumarin unit with the symmetry-related part is 74.78 (14)°. One of the meth-oxy groups attached to the coumarin unit is considerably twisted, making an angle of 87.17 (17)° with respect to the coumarin unit; the other is twisted by 0.66 (19)°. No classical hydrogen bonds are found in the sturcture; only a weak C-H⋯π inter-action and short intra-molecular O⋯O contacts [2.683 (2)-2.701 (2) Å] are observed.
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