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Updated: Jun 1, 2026
08:43
Protocol for the Synthesis of Ortho-trifluoromethoxylated Aniline Derivatives
Published on: January 19, 2016
4-Meth-oxy-N'-(2-methoxy-benzyl-idene)benzohydrazide
1Department of Chemistry, Baicheng Normal College, Baicheng 137000, People's Republic of China.
Summary
This study details the crystal structure of a C(16)H(16)N(2)O(3) compound, revealing a specific molecular geometry and intermolecular interactions. The findings highlight the compound
Area of Science:
- Crystallography
- Organic Chemistry
- Molecular Structure
Background:
- Understanding molecular arrangements is crucial in chemistry.
- Crystal structure analysis provides insights into intermolecular forces.
Purpose of the Study:
- To determine the precise three-dimensional structure of the C(16)H(16)N(2)O(3) compound.
- To investigate the intermolecular interactions within the crystal lattice.
Main Methods:
- Single-crystal X-ray diffraction was employed.
- Analysis of bond lengths, angles, and torsion angles.
- Identification of hydrogen bonding networks.
Main Results:
- The compound exhibits an E configuration around the C=N bond.
- Two benzene rings are inclined at an angle of 75.4(2)°.
- Intermolecular N-H⋯O hydrogen bonds form chains along the c axis.
Conclusions:
- The crystal packing is stabilized by a network of hydrogen bonds.
- The determined structure provides a foundation for further studies on this class of compounds.
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