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Updated: May 31, 2026

Chemical Precipitation Method for the Synthesis of Nb2O5 Modified Bulk Nickel Catalysts with High Specific Surface Area
08:13

Chemical Precipitation Method for the Synthesis of Nb2O5 Modified Bulk Nickel Catalysts with High Specific Surface Area

Published on: February 19, 2018

Li(2)Ca(1.5)Nb(3)O(10) from X-ray powder data.

Bai-Chuan Zhu, Kai-Bin Tang

    Acta Crystallographica. Section E, Structure Reports Online
    |July 15, 2011
    PubMed
    Summary
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    Researchers synthesized lithium calcium niobium oxide, Li(2)Ca(1.5)Nb(3)O(10), using solid-state reactions. The study details its unique triple-layer perovskite structure with specific atomic arrangements.

    Area of Science:

    • Solid-state chemistry
    • Materials science
    • Crystallography

    Background:

    • Lithium calcium niobium oxide (Li(2)Ca(1.5)Nb(3)O(10)) is a complex oxide material.
    • Understanding the crystal structure of novel oxides is crucial for potential applications.

    Purpose of the Study:

    • To synthesize lithium calcium niobium oxide via a conventional solid-state reaction.
    • To characterize the crystal structure of the synthesized Li(2)Ca(1.5)Nb(3)O(10).

    Main Methods:

    • Conventional solid-state reaction for synthesis.
    • X-ray diffraction or similar crystallographic techniques for structural analysis (implied).

    Main Results:

    • Successful synthesis of Li(2)Ca(1.5)Nb(3)O(10) was achieved.

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    Chemical Precipitation Method for the Synthesis of Nb2O5 Modified Bulk Nickel Catalysts with High Specific Surface Area
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  • The crystal structure features triple-layer perovskite slabs composed of corner-sharing NbO(6) octahedra.
  • Lithium ions inter-leave these slabs, and calcium cations partially occupy A sites (75% occupancy).
  • All eight atoms in the asymmetric unit occupy special crystallographic positions.

    • Conclusions:

    • The study reports the successful synthesis and structural characterization of a novel lithium calcium niobium oxide.
    • The detailed structural information provides a basis for further investigation into its properties and potential uses.