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Coordination compounds and complexes exhibit different colors, geometries, and magnetic behavior, depending on the metal atom/ion and ligands from which they are composed. In an attempt to explain the bonding and structure of coordination complexes, Linus Pauling proposed the valence bond theory, or VBT, using the concepts of hybridization and the overlapping of the atomic orbitals. According to VBT, the central metal atom or ion (Lewis acid) hybridizes to provide empty orbitals of suitable...
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Related Experiment Video

Updated: May 31, 2026

Synthesis of In37P20(O2CR)51 Clusters and Their Conversion to InP Quantum Dots
08:21

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Published on: May 7, 2019

A mixed indium-iron lithium diphosphate, In(0.51)Fe(0.49)LiP(2)O(7).

Hafid Zouihri, Mohamed Saadi, Boujemaa Jaber

    Acta Crystallographica. Section E, Structure Reports Online
    |July 15, 2011
    PubMed
    Summary
    This summary is machine-generated.

    The crystal structure of indium-iron lithium diphosphate reveals a 3D network with M(III)O(6) octahedra and P(2)O(7) groups, forming tunnels housing Li(+) ions. This compound is part of a solid solution series.

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    Area of Science:

    • Solid-state chemistry
    • Inorganic chemistry
    • Crystallography

    Background:

    • The A(I)FeP(2)O(7) family of diphosphates exhibits isotypic structures.
    • Understanding structure-property relationships in mixed-metal diphosphates is crucial for materials science.

    Purpose of the Study:

    • To elucidate the crystal structure of In(0.51)Fe(0.49)LiP(2)O(7).
    • To characterize its place within the LiFeP(2)O(7)-LiInP(2)O(7) solid solution series.

    Main Methods:

    • Single-crystal or powder X-ray diffraction analysis was likely employed to determine the atomic arrangement.
    • Structural characterization involved analyzing the coordination of metal ions and the connectivity of polyhedra.

    Main Results:

    • The structure features a 3D framework of (In(III)/Fe(III))O(6) octahedra and P(2)O(7) groups.
    • Infinite chains of [M(III)P(2)O(11)] run along the a-axis, linked to form heptagonal tunnels.
    • Lithium (Li+) ions occupy off-centered positions within these tunnels.

    Conclusions:

    • In(0.51)Fe(0.49)LiP(2)O(7) represents a specific composition within a continuous solid solution.
    • The structural framework and ion localization provide insights into diphosphate materials.