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Na(3)DyCl(6).

Christian M Schurz, Gerd Meyer, Thomas Schleid

    Acta Crystallographica. Section E, Structure Reports Online
    |July 15, 2011
    PubMed
    Summary
    This summary is machine-generated.

    Single crystals of tris-odium hexa-chloridodysprosate (Na(3)DyCl(6)) were synthesized. This compound exhibits a monoclinic structure, isotypic with cryolite, featuring isolated dysprosium chloride octahedra and distinct sodium cation coordination environments.

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    Area of Science:

    • Inorganic Chemistry
    • Solid-State Chemistry
    • Crystallography

    Background:

    • Dysprosium chloride and sodium chloride are common inorganic compounds.
    • The Na(3)MCl(6) series, where M represents various lanthanides, scandium, or yttrium, is known to form cryolite-type structures.
    • Understanding the structural variations in these compounds is crucial for materials science.

    Purpose of the Study:

    • To characterize the crystal structure of tris-odium hexa-chloridodysprosate (Na(3)DyCl(6)).
    • To investigate the coordination environment of dysprosium and sodium cations within the crystal lattice.
    • To compare the determined structure with known isotypic compounds.

    Main Methods:

    • Single crystal X-ray diffraction was used to determine the crystal structure.
    • Synthesis of the compound was achieved as a byproduct of reactions involving dysprosium(III) chloride and sodium chloride.
    • Structural analysis involved identifying coordination polyhedra and symmetry elements.

    Main Results:

    • Single crystals of Na(3)DyCl(6) were successfully obtained.
    • The compound crystallizes in a monoclinic structure, isotypic with cryolite (Na(3)AlF(6)).
    • The structure consists of isolated [DyCl(6)](3-) octahedra and two types of sodium coordination: one Na(+) in an [NaCl(6)](5-) octahedron and another Na(+) in a distorted [NaCl(7)](6-) trigonal prism.

    Conclusions:

    • Tris-odium hexa-chloridodysprosate (Na(3)DyCl(6)) adopts a cryolite-type structure.
    • The distinct coordination environments of the sodium cations contribute to the overall crystal architecture.
    • The findings provide insights into the structural diversity within the Na(3)MCl(6) series.