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Updated: May 30, 2026

Continuous Flow Chemistry: Reaction of Diphenyldiazomethane with p-Nitrobenzoic Acid
Published on: November 15, 2017
(S)-2-[1-(4-Bromo-phen-yl)-1-hy-droxy-ethyl]-5,5-dimethyl-1,3,2-dioxaphos-phinane 2-oxide
Chubei Wang1, Hao Peng, Hongwu He
1Key Laboratory of Pesticide and Chemical Biology, College of Chemistry, Central China Normal University, Wuhan 430079, People's Republic of China .
Abstract:
In the crystal structure of the title mol-ecule, C(13)H(18)BrO(4)P, the phospho-nate ring adopts a chair conformation. Mol-ecules are linked by an O-H⋯O hydrogen bond [O⋯O = 2.780 (3) Å] to form chains parallel to the c axis. Two C-H⋯O inter-actions help to stabilize the crystal structure.
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