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Related Concept Videos

Preparation and Reactions of Sulfides02:26

Preparation and Reactions of Sulfides

Sulfides are the sulfur analog of ethers, just as thiols are the sulfur analog of alcohol. Like ethers, sulfides also consist of two hydrocarbon groups bonded to the central sulfur atom. Depending upon the type of groups present, sulfides can be symmetrical or asymmetrical. Symmetrical sulfides can be prepared via an SN2 reaction between 2 equivalents of an alkyl halide and one equivalent of sodium sulfide.

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Related Experiment Video

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Insights into the Interactions of Amino Acids and Peptides with Inorganic Materials Using Single-Molecule Force Spectroscopy
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Trimeth-yl(triphenyl-meth-oxy)silane.

Sumati Anthal, Bubun Banerjee, Goutam Brahmacharia

    Acta Crystallographica. Section E, Structure Reports Online
    |February 21, 2012
    PubMed
    Summary

    This study details the molecular structure of a C(22)H(24)OSi compound, revealing specific bond angles and crystal packing. Weak van der Waals forces and π-π interactions govern its solid-state arrangement.

    Area of Science:

    • Crystallography
    • Organic Chemistry
    • Materials Science

    Background:

    • Understanding molecular geometry and intermolecular forces is crucial for predicting material properties.
    • Crystal structure analysis provides fundamental insights into how molecules arrange in the solid state.

    Purpose of the Study:

    • To elucidate the detailed molecular geometry of the title compound C(22)H(24)OSi.
    • To investigate the intermolecular interactions, including π-π stacking and van der Waals forces, present in the crystal lattice.

    Main Methods:

    • Single-crystal X-ray diffraction was employed to determine the three-dimensional structure.
    • Analysis of bond angles, dihedral angles, and inter-centroid distances provided insights into molecular conformation and packing.

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    Main Results:

    • The Si-O-C angle was determined to be 139.79(11)°.
    • Face-to-face π-π interactions between phenyl rings were observed with a centroid separation of 4.194(1) Å and interplanar spacing of 3.474 Å.
    • The phenyl groups exhibited dihedral angles between 80.49(8)° and 81.53(8)°, indicating a nearly perpendicular arrangement, with only weak intermolecular van der Waals interactions present.

    Conclusions:

    • The molecular structure is characterized by specific bond angles within the trimethyl-sil-yloxy and triphenyl-meth-oxy groups.
    • The crystal packing is influenced by significant π-π interactions and weak van der Waals forces.
    • The study provides a comprehensive structural characterization of the C(22)H(24)OSi molecule in the solid state.