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Updated: May 24, 2026

08:43
Molten-Salt Synthesis of Complex Metal Oxide Nanoparticles
Published on: October 27, 2018
A strategy for the synthesis of mesostructured metal oxides with lower oxidation states
Harun Tüysüz1, Claudia Weidenthaler, Ferdi Schüth
1Max-Planck-Institut für Kohlenforschung, Kaiser-Wilhelm-Platz 1, 45470 Mülheim an der Ruhr, Germany.
Chemistry (Weinheim an Der Bergstrasse, Germany)
|March 14, 2012
Abstract:
A detailed study on the pseudomorphic conversion of ordered mesoporous Co(3)O(4) and ferrihydrite into CoO and Fe(3)O(4), respectively, by using alcohol/water vapor as a gentle reducing agent is described. The reduction conditions for the transformation were optimized. In addition, the first one-pot synthesis of mesostructured CoO by using nanocasting with cubic ordered silica as a hard template is demonstrated.
