Search research articles

ABOUT JoVE

Overview Leadership Blog JoVE Help Center

AUTHORS

Publishing Process Editorial Board Scope & Policies Peer Review FAQ Submit

LIBRARIANS

Testimonials Subscriptions Access Resources Library Advisory Board FAQ

RESEARCH

JoVE Journal Methods Collections JoVE Encyclopedia of Experiments Archive

EDUCATION

JoVE Core JoVE Business JoVE Science Education JoVE Lab Manual Faculty Resource Center Faculty Site

Terms & Conditions of Use

Related Concept Videos

You might also read

Related Articles

Articles linked to this work by shared authors, journal, and citation graph.

Sort by

Same author

Platinum(IV) Complexes of the 1,3,5-Triamino Analogue of the Biomolecule Cis-Inositol Designed as Innovative Antineoplastic Drug Candidates.

Pharmaceutics·2022

Same author

Crystal structure and Hirshfeld surface analysis of tris-(2,2'-bi-pyridine)-nickel(II) bis-(1,1,3,3-tetra-cyano-2-eth-oxy-propenide) dihydrate.

Acta crystallographica. Section E, Crystallographic communications·2019

Same author

HBr or not HBr? That is the question: crystal structure of 6-hydroxy-1,4-diazepane-1,4-diium dibromide redetermined.

Acta crystallographica. Section C, Structural chemistry·2019

Same author

Crystal structure of

Acta crystallographica. Section E, Crystallographic communications·2018

Same author

T-Symmetrical Icosahedra: A New Type of Chirality in Metal Complexes.

Angewandte Chemie (International ed. in English)·2018

Same author

Hafnium-Based Contrast Agents for X-ray Computed Tomography.

Inorganic chemistry·2017

Same journal

Crystal structure of 1-(piperidin-1-yl)butane-1,3-dione.

Acta crystallographica. Section E, Structure reports online·2015

Same journal

Crystal structure of methyl 1-methyl-3,5-diphenyl-7-tosyl-3,6,7,11b-tetra-hydro-pyrazolo-[4',3':5,6]pyrano[3,4-c]quinoline-5a(5H)-carboxyl-ate.

Acta crystallographica. Section E, Structure reports online·2015

Same journal

Crystal structure of 4-amino-1-(4-methyl-benz-yl)pyridinium bromide.

Acta crystallographica. Section E, Structure reports online·2015

Same journal

Crystal structure of (Z)-3-benz-yloxy-6-[(2-hy-droxy-anilino)methyl-idene]cyclo-hexa-2,4-dien-1-one.

Acta crystallographica. Section E, Structure reports online·2015

Same journal

Crystal structure of bis-(1-benzyl-1H-1,2,4-triazole) perchloric acid monosolvate.

Acta crystallographica. Section E, Structure reports online·2015

Same journal

Crystal structure of 2-(di-phenyl-phos-phanyl)phenyl 4-(hy-droxy-meth-yl)benzoate.

Acta crystallographica. Section E, Structure reports online·2015

See all related articles

Search research articles

Related Experiment Video

Updated: May 24, 2026

Synthesis of Indoxyl-glycosides for Detection of Glycosidase Activities

Synthesis of Indoxyl-glycosides for Detection of Glycosidase Activities

Published on: May 27, 2015

4,6-Dinitro-pyrogallol.

Christian Neis¹, Günter J Merten, Kaspar Hegetschweiler

¹Fachrichtung Chemie, Universität des Saarlandes, Postfach 151150, D-66041 Saarbrücken, Germany.

Acta Crystallographica. Section E, Structure Reports Online

|March 14, 2012

Summary

This summary is machine-generated.

This study details the molecular structure of C(6)H(4)N(2)O(7), revealing specific nitro group tilts and extensive hydrogen bonding. Crystal packing analysis identified short oxygen-oxygen distances between nitro groups.

More Related Videos

Isolation of Peritoneum-derived Mast Cells and Their Functional Characterization with Ca2+-imaging and Degranulation Assays

Isolation of Peritoneum-derived Mast Cells and Their Functional Characterization with Ca²⁺-imaging and Degranulation Assays

Published on: July 4, 2018

Synthesis of pH Dependent Pyrazole, Imidazole, and Isoindolone Dipyrrinone Fluorophores using a Claisen-Schmidt Condensation Approach

Synthesis of pH Dependent Pyrazole, Imidazole, and Isoindolone Dipyrrinone Fluorophores using a Claisen-Schmidt Condensation Approach

Published on: June 10, 2021

Related Experiment Videos

Last Updated: May 24, 2026

Synthesis of Indoxyl-glycosides for Detection of Glycosidase Activities

Synthesis of Indoxyl-glycosides for Detection of Glycosidase Activities

Published on: May 27, 2015

Isolation of Peritoneum-derived Mast Cells and Their Functional Characterization with Ca2+-imaging and Degranulation Assays

Isolation of Peritoneum-derived Mast Cells and Their Functional Characterization with Ca²⁺-imaging and Degranulation Assays

Published on: July 4, 2018

Synthesis of pH Dependent Pyrazole, Imidazole, and Isoindolone Dipyrrinone Fluorophores using a Claisen-Schmidt Condensation Approach

Synthesis of pH Dependent Pyrazole, Imidazole, and Isoindolone Dipyrrinone Fluorophores using a Claisen-Schmidt Condensation Approach

Published on: June 10, 2021

Area of Science:

Crystallography
Organic Chemistry
Molecular Structure

Background:

Understanding the precise arrangement of atoms and intermolecular forces is crucial in organic chemistry.
Detailed structural analysis provides insights into chemical properties and reactivity.

Purpose of the Study:

To elucidate the crystal structure of the molecule C(6)H(4)N(2)O(7).
To investigate the spatial orientation of nitro groups and the role of hydroxyl groups in hydrogen bonding.
To analyze intermolecular interactions within the crystal lattice.

Main Methods:

Single-crystal X-ray diffraction was employed to determine the molecular and crystal structure.
Analysis of bond lengths, bond angles, and hydrogen bonding networks.

Main Results:

The nitro groups are tilted at 11.2° and 10.9° relative to the aromatic ring.
All three hydroxyl groups participate in bifurcated intra- and intermolecular hydrogen bonds.
Short O⋯O distances (2.823 Å) were observed between nitro group oxygen atoms in the crystal packing.

Conclusions:

The structural data provides a detailed understanding of the molecule's conformation and intermolecular interactions.
The observed hydrogen bonding and short O⋯O distances likely influence the molecule's stability and reactivity.
This study contributes to the knowledge of nitroaromatic compounds and their solid-state behavior.