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Updated: May 22, 2026

Continuous Flow Chemistry: Reaction of Diphenyldiazomethane with p-Nitrobenzoic Acid
Published on: November 15, 2017
2-Hy-droxy-N'-[2-(6-meth-oxy-naphthalen-2-yl)propano-yl]benzohydrazide
Abstract:
In the title compound, C(21)H(20)N(2)O(4), the naphthalene ring system makes a dihedral angle of 84.5 (3)° with the benzene ring, and the -C(=O)-N(H)-N(H)-C(=O)- torsion angle is 70.7 (7)°, so that the mol-ecule is twisted. An S(6) ring motif is formed via an intra-molecular O-H⋯O hydrogen bond. In the crystal, mol-ecules are linked by N-H⋯O and C-H⋯O hydrogen bonds into supra-molecular layers in the ab plane.
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