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Updated: May 21, 2026
06:34
Synthesis of Antiviral Tetrahydrocarbazole Derivatives by Photochemical and Acid-catalyzed C-H Functionalization via Intermediate Peroxides (CHIPS)
Published on: June 20, 2014
N-(4-Bromo-phen-yl)-3,4,5-trimeth-oxy-benzamide
1College of Chemical Engineering, Nanjing Forestry University, Nanjing 210037, People's Republic of China.
Summary
This study details the crystal structure of a novel organic compound, C(16)H(16)BrNO(4). Molecular analysis reveals a specific dihedral angle between aromatic rings and intermolecular hydrogen bonding in its crystalline form.
Area of Science:
- Crystallography
- Organic Chemistry
- Molecular Structure
Background:
- Understanding the three-dimensional arrangement of atoms in organic compounds is crucial for predicting their properties.
- Intermolecular forces, such as hydrogen bonds, significantly influence crystal packing and material characteristics.
Purpose of the Study:
- To elucidate the crystal structure of the title compound, C(16)H(16)BrNO(4).
- To analyze the spatial arrangement and intermolecular interactions within the crystal lattice.
Main Methods:
- Single-crystal X-ray diffraction was employed to determine the molecular and crystal structure.
- Analysis of bond lengths, bond angles, and dihedral angles provided detailed structural information.
Main Results:
- The dihedral angle between the two aromatic rings in C(16)H(16)BrNO(4) was determined to be 67.51°.
- Molecules are organized into chains via N-H⋯O hydrogen bonds between amide functional groups.
Conclusions:
- The study provides precise structural data for C(16)H(16)BrNO(4).
- The identified hydrogen bonding pattern dictates the supramolecular architecture in the solid state.
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