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Synthesis of Ligand-free CdS Nanoparticles within a Sulfur Copolymer Matrix
Published on: May 1, 2016
Facile synthesis of cysteine and triethanolamine capped CdTe nanoparticles
Nhlakanipho Mntungwa1, Viswanadha Srirama Rajasekhar Pullabhotla, Neerish Revaprasadu
1Department of Chemistry, University of Zululand, KwaDlangezwa 3886, South Africa.
Abstract:
Cysteine and triethanolamine capped CdTe nanoparticles have been synthesized using a simple aqueous solution based method. This method involves the reaction of tellurium powder with sodium borohydride (NaBH(4)) in water to produce telluride ions (Te(2-)), followed by the simultaneous addition of an aqueous solution of cadmium chloride or other cadmium source (acetate, carbonate and nitrate) and solution of L-cysteine ethyl ester hydrochloride or triethanolamine. The effect of capping agent on the size, structure and morphology of the as-synthesized nanoparticles was investigated. The particles were characterized using optical spectroscopy, transmission electron microscopy (TEM), high-resolution TEM (HRTEM), X-ray diffraction (XRD) and Fourier transform infrared (FT-IR) spectroscopy.

