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Updated: May 16, 2026

Energy Dispersive X-ray Tomography for 3D Elemental Mapping of Individual Nanoparticles
Published on: July 5, 2016
Three-dimensional characterization of iron oxide (α-Fe2O3) nanoparticles: application of a compressed sensing
Niven Monsegue1, Xin Jin, Takuya Echigo
1Institute for Critical Technology and Applied Science, Virginia Tech, Blacksburg, VA 24061, USA. nmonsegu@vt.edu
Abstract:
In this article, we demonstrate the application of a new compressed sensing three-dimensional reconstruction algorithm for electron tomography that increases the accuracy of morphological characterization of nanostructured materials such as nanocrystalline iron oxide particles. A powerful feature of the algorithm is an anisotropic total variation norm for the L1 minimization during algebraic reconstruction that effectively reduces the elongation artifacts caused by limited angle sampling during electron tomography. The algorithm provides faithful morphologies that have not been feasible with existing techniques.
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