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Diisopropylammonium chloride.

P Prince1, J A Miller, F R Fronczek

  • 1Department of Chemistry, Louisiana State University, Baton Rouge 70803-1804.

Acta Crystallographica. Section C, Crystal Structure Communications
|February 15, 1990
PubMed
Summary
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This study details the crystal structure of a compound, revealing specific hydrogen bonding interactions between nitrogen and chlorine atoms. These findings elucidate the molecular arrangement and bonding within the crystalline solid.

Area of Science:

  • Crystallography
  • Solid-state Chemistry

Background:

  • Understanding molecular interactions is crucial in solid-state chemistry.
  • Hydrogen bonding plays a significant role in crystal lattice formation and stability.

Purpose of the Study:

  • To determine the crystal structure of C6H16N+.Cl-.
  • To investigate the hydrogen bonding network within the crystal.

Main Methods:

  • Single-crystal X-ray diffraction was employed.
  • The crystal structure was solved and refined using standard crystallographic techniques.

Main Results:

  • The compound crystallizes in an orthorhombic system (P2(1)2(1)2(1)) with specific lattice parameters.
  • Detailed analysis revealed hydrogen bonds between nitrogen (N) and chlorine (Cl) atoms, with N--H...Cl distances and angles precisely measured.

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  • Each chlorine atom participates in two hydrogen bonds, and the cation exhibits approximate twofold symmetry.

    • Conclusions:

    • The crystal structure of C6H16N+.Cl- has been fully characterized.
    • The identified hydrogen bonding network provides insights into the intermolecular forces governing the solid-state structure.