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Direct quantification of ordering at a solid-liquid interface using aberration corrected transmission electron

Maria Gandman1, Yaron Kauffmann, Christoph T Koch

  • 1Department of Materials Science and Engineering, Technion-Israel Institute of Technology, Haifa 32000, Israel.

Physical Review Letters
|March 12, 2013
PubMed
Summary
This summary is machine-generated.

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Liquid aluminum shows ordered interfaces with sapphire, with ordering degree varying by sapphire facet. This study confirms liquid ordering at interfaces using advanced microscopy techniques.

Area of Science:

  • Materials Science
  • Surface Science
  • Nanotechnology

Background:

  • Understanding liquid-solid interfaces is crucial for materials processing and nanotechnology.
  • The atomic structure of liquid metals at interfaces with oxides influences wetting and interfacial reactions.

Purpose of the Study:

  • To investigate the atomic-level ordering of liquid aluminum at interfaces with various sapphire (Al2O3) crystallographic planes.
  • To quantitatively correlate the degree of liquid ordering with specific sapphire facet orientations.

Main Methods:

  • Aberration-corrected in situ transmission electron microscopy (TEM) was employed for high-resolution imaging.
  • Quantitative analysis of contrast delocalization in TEM images was performed to infer liquid density perturbations.

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Related Experiment Videos

Last Updated: May 13, 2026

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10:25

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Published on: September 14, 2018

Revealing Dynamic Processes of Materials in Liquids Using Liquid Cell Transmission Electron Microscopy
07:37

Revealing Dynamic Processes of Materials in Liquids Using Liquid Cell Transmission Electron Microscopy

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Main Results:

  • The study confirmed the presence of ordered structures in liquid aluminum at the interface with sapphire.
  • The degree of liquid ordering was found to be dependent on the sapphire facet plane.
  • A specific order of decreasing liquid order was established: (0006) > (1210) > (1012) ≥ (1014).

Conclusions:

  • Liquid aluminum exhibits significant interfacial ordering when in contact with sapphire.
  • The crystallographic orientation of the sapphire surface dictates the extent of this liquid-state ordering.