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Green synthesized nickel nanoparticles modified electrode in ionic liquid medium and its application towards

Rajendran Suresh Babu1, Pandurangan Prabhu, Sangilimuthu Sriman Narayanan

  • 1Department of Analytical Chemistry, School of Chemical Sciences, University of Madras, Guindy Campus, Chennai 600 025, Tamil Nadu, India.

Talanta
|April 27, 2013
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Precipitation Gravimetry01:03

Precipitation Gravimetry

Precipitation gravimetry is based on converting an analyte into a sparingly soluble precipitate, which is separated by filtration and weighed. An ideal precipitate should be pure, insoluble, of known composition, and easily filtered from the reaction mixture.
In determining nickel by gravimetric analysis, a precipitant of ethanolic dimethylglyoxime is added to a hot nickel salt solution. This is quickly followed by the dropwise addition of dilute ammonia solution until precipitation occurs. A...