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Updated: May 11, 2026

Quantitative Hardness Measurement by Instrumented AFM-indentation
Published on: November 22, 2016
Formation of nanostructure and nano-hardness characterization on the meso-scale workpiece by a novel laser indirect
1School of Mechanical Engineering, Jiangsu University, Zhenjiang 212013, People's Republic of China.
Abstract:
The meso-scale workpiece with greatly enhanced mechanical properties is potential to be widely used in the electronics productions and micro-electro mechanical systems. In this study, it demonstrates that the meso-scale cup-shape workpiece with good geometry can be obtained by a novel laser indirect shock forming method. After the forming process, the mechanical properties and microstructures of the formed workpiece were characterized. By transmission electron microscope observation, it was found that a mixed refined microstructure consisting of nano-scale twins embedded in nano-sized grains was produced at the center of the formed sample. Formation of these nanograins could be mainly attributed to two mechanisms: twin-twin intersections and twin∕matrix lamellae fragmentation. By nanoindentation tests, it reveals that the hardness of the sample has increased greatly after laser shock forming and the hardness increases with the laser energy. The elevated hardness originates from a considerable number of nano-scale twins and nanograins, which possess a pretty high strength due to the significant effects of grain boundary strengthening and twin boundary strengthening.

