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Synthesis of functional carbon nanospheres by a composite-molten-salt method and amperometric sensing of hydrogen
Xue Wang1, Chenguo Hu, Yufeng Xiong
1Department of Applied Physics, Chongqing University, Chongqing 400044, PR China.
Abstract:
Functional carbon nanospheres have been synthesized from analytically pure glucose by a composite-molten-salt (CMS) method. Field emission scanning electron microscopy, transmission electron microscopy, Raman and Fourier transformation infra-red spectroscopy indicate the carbon nanospheres are solid, bond hybridisation (sp2/sp3) and with many functional groups on their surfaces. Amperometric sensor based on the synthesized carbon nanospheres have been fabricated without pretreatment or modification. The detection of hydrogen peroxide exhibits high sensitivity and good selectivity. The electrochemical measurement of these nanospheres demonstrates much superior performance to those of the carbon nanospheres synthesized by hydrothermal method.
