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Characterization of Ultra-fine Grained and Nanocrystalline Materials Using Transmission Kikuchi Diffraction
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Understanding ultrafine nanodiamond formation using nanostructured explosives.

Vincent Pichot1, Benedikt Risse, Fabien Schnell

  • 1NS3E «Nanomatériaux pour les Systèmes Sous Sollicitations Extrêmes» UMR ISL-CNRS-UDS 3208, French-German Research Institute of Saint-Louis, 5 Rue du Général Cassagnou, 68301 Saint-Louis, France.

Scientific Reports
|July 9, 2013
PubMed
Summary

Nanostructured explosives enable the synthesis of smaller detonation nanodiamonds. This breakthrough offers new insights into nanodiamond formation mechanisms and particle size control.

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Research and Development of High-performance Explosives
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Area of Science:

  • Materials Science
  • Nanotechnology
  • Chemistry

Background:

  • Detonation synthesis is a bottom-up approach for creating novel materials.
  • Nanodiamond particles can be synthesized from high-explosive molecules containing carbon.
  • Trinitrotoluene (TNT) and hexogen (RDX) are commonly used explosives for nanodiamond synthesis.

Purpose of the Study:

  • To investigate the effect of nanostructured explosive charges on nanodiamond synthesis.
  • To gain a deeper understanding of the mechanisms governing nanodiamond formation.
  • To explore methods for controlling nanodiamond particle size.

Main Methods:

  • Utilizing nanostructured explosive charges for detonation synthesis.
  • Analyzing the resulting nanodiamond particles for size and morphology.
  • Comparing synthesis outcomes with conventional microstructured charges.

Main Results:

  • Nanostructured explosive charges yield smaller detonation nanodiamonds compared to conventional methods.
  • The nanoscale discontinuity of the explosive is identified as the critical factor influencing diamond particle size.
  • Controlling nanodiamond size using microstructured charges was found to be ineffective.

Conclusions:

  • Nanostructured explosives offer a viable route to producing smaller nanodiamonds.
  • Understanding the role of explosive discontinuity is key to controlling nanodiamond characteristics.
  • This research advances the field of detonation synthesis for nanomaterials.